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Beilstein J. Org. Chem. 2020, 16, 616–620, doi:10.3762/bjoc.16.57
Graphical Abstract
Scheme 1: Retrosynthesis of (+)-disparlure (1), (−)-disparlure (3), (+)-monachalure (2), and (−)-monachalure (...
Scheme 2: Isomerization of trans-2,3-butanediacetals 9–11 to cis-2,3-butanediacetals 12–14.
Scheme 3: Synthesis of diol 17 and its subsequent modifications.
Scheme 4: Synthesis of (+)-disparlure (1) and (+)-monachalure (2).
Scheme 5: Synthesis of (−)-disparlure (3) and (−)-monachalure (4).